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The key ion species used at NCEM is Ga+, with an extra minimal-Vitality Ar+ ion source available over the FIB or using the Fischionne NanoMill just after FIB planning. Additionally, iodine gasoline-assisted etching is obtainable. When a gasoline is introduced close to the floor of the sample throughout milling, the sputtering yield can increase dependant upon the chemistry between the fuel and the sample. This ends in less redeposition and much more successful milling.

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six. If specimens usually are not self supporting, copper grids are generally enough to 500C. For focus on temperatures previously mentioned 500C, molybdenum grids are essential. Gatan G-one substantial temperature epoxy stays intact at temperatures in surplus of 1000C.

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